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  3. Chemistry; Chem Sci/Eng

oiled out

Russian translation: выделится в виде масла (маслянистой жидкости)

21:52 Mar 22, 2017
English to Russian translations [PRO]
Tech/Engineering - Chemistry; Chem Sci/Eng
English term or phrase: oiled out
Crystal seeds were obtained in the following manner: to a solution of (S)-7-ethyl-N-((R)-1-(4-(ethylsulfonyl)phenyl)-2-hydroxyethyl)-6-((trans-4-(trifluoromethyl)cyclohexyl)methyl)-6,7-dihydro-5H-pyrrolo[3,4-b]pyridine-3-carboxamide (59.7 mg, 0.11 mmol) in ethyl acetate (0.5 mL) was added methanesulfonic acid (19.8 mg, 1.95 eq) dropwise. The salt ***oiled out***. After decanting the top layer of ethyl acetate, the residue was dried over vacuum to remove any residual ethyl acetate. The residue was then redissolved in EtOH (~5 mL) by warming the solution up to give a clear solution. Crystals crashed out after standing at rt overnight (17.5 mg, 25%)
Palladium
United States
Local time: 00:44
Russian translation:выделится в виде масла (маслянистой жидкости)
Explanation:
.....
Selected response from:

mikhailo
Local time: 00:44
Grading comment
4 KudoZ points were awarded for this answer



Summary of answers provided
5 +2выделится в виде масла (маслянистой жидкости)
mikhailo
Summary of reference entries provided
см.
Andrey Svitanko

  

Answers


1 hr   confidence: Answerer confidence 5/5 peer agreement (net): +2
выделится в виде масла (маслянистой жидкости)


Explanation:
.....

mikhailo
Local time: 00:44
Works in field
Native speaker of: Native in RussianRussian, Native in BelarusianBelarusian
PRO pts in category: 79

Peer comments on this answer (and responses from the answerer)
agree  Leila Usmanova
4 hrs
agree  Mikhail Yanchenko
13 hrs
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Reference comments


1 hr
Reference: см.

Reference information:
http://www.chem.ualberta.ca/~iip/OrgLabBookS/v.lab/isolation...

Oiled out or Oiling out

Definition: A condition when a compound forms an oil instead of a precipitate or crystals;
occurs most frequently with low melting solids,
occurs also during purification of low melting point solids using mixed solvent recrystallization.

Andrey Svitanko
Poland
Specializes in field
Native speaker of: Native in RussianRussian
PRO pts in category: 449
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